Operando isotope selective ammonia quantification in nitrogen reduction studies via gas chromatography-mass spectrometry

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Abstract

Rapid advances in electrocatalytic ammonia synthesis are impeded by laborious detection methods commonly used in the field and by constant risk of external contaminations, which generates misleading false positives. We developed a facile real-time GC-MS method for sensitive isotope NH3 quantification, requiring no external sample manipulations. This method ensures high detection reliability paramount to accelerate (electro-)catalyst screening.
Original languageEnglish
Pages (from-to)1945-1949
JournalSustainable Energy & Fuels
Volume6
Issue number8
DOIs
Publication statusPublished - 2022

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