TY - JOUR
T1 - Resin Transfer molding of High-Fluidity Polyamide-6 with modified Glass-Fabric preforms
AU - Gomez, Colin
AU - Salvatori, Damiano
AU - Caglar, Baris
AU - Trigueira, Robin
AU - Orange, Gilles
AU - Michaud, Véronique
PY - 2021
Y1 - 2021
N2 - In Resin Transfer Molding (RTM), resin precursors of thermoset or, more recently, thermoplastic polymers are generally employed, raising issues related to the chemical reaction taking place during and after part processing. In this study, already polymerized polyamide-6 with low melt-viscosity (~30 Pa·s at 280 °C), is injected at low pressure (<30 bar) in a custom-made mold, so as to impregnate glass fabric preforms via in-plane impregnation. Composite plates were produced using interply spacers acting as flow-enhancers. A three-step impregnation strategy, involving fast in-plane resin injection, a successive saturation step through transverse flow, followed by further micro-saturation caused by the collapse of the spacers, ensured industrially relevant impregnation kinetics. The influence of the spacer, the saturation time, pressure and temperature on the process kinetics and part quality were evaluated with three-point bending tests as well as microstructural analyses. Optimum processing parameters were identified and scaled up for a given part geometry.
AB - In Resin Transfer Molding (RTM), resin precursors of thermoset or, more recently, thermoplastic polymers are generally employed, raising issues related to the chemical reaction taking place during and after part processing. In this study, already polymerized polyamide-6 with low melt-viscosity (~30 Pa·s at 280 °C), is injected at low pressure (<30 bar) in a custom-made mold, so as to impregnate glass fabric preforms via in-plane impregnation. Composite plates were produced using interply spacers acting as flow-enhancers. A three-step impregnation strategy, involving fast in-plane resin injection, a successive saturation step through transverse flow, followed by further micro-saturation caused by the collapse of the spacers, ensured industrially relevant impregnation kinetics. The influence of the spacer, the saturation time, pressure and temperature on the process kinetics and part quality were evaluated with three-point bending tests as well as microstructural analyses. Optimum processing parameters were identified and scaled up for a given part geometry.
KW - A. Thermoplastic resin
KW - B. Polymer-matrix composites (PMCs)
KW - E. Preforming
KW - E. Resin transfer molding (RTM)
UR - http://www.scopus.com/inward/record.url?scp=85106276808&partnerID=8YFLogxK
U2 - 10.1016/j.compositesa.2021.106448
DO - 10.1016/j.compositesa.2021.106448
M3 - Article
AN - SCOPUS:85106276808
VL - 147
JO - Composites Part A: Applied Science and Manufacturing
JF - Composites Part A: Applied Science and Manufacturing
SN - 1359-835X
M1 - 106448
ER -